MSO: NMR spectra

References

Spectrum

	Authors:	Paillaud, J.-L., Caullet, P., Schreyeck, L. and Marler, B.
	Title:	Mu-13: a new AlPO₄ prepared with 4,13-diaza-18-crown-6 as a structuring agent
	Reference:	Microporous Mesoporous Mat., 42, 177-189 (2001)
	Figure:	Figure 7

Peak Assignment

	Authors:	Paillaud, J.-L., Caullet, P., Schreyeck, L. and Marler, B.
	Title:	Mu-13: a new AlPO₄ prepared with 4,13-diaza-18-crown-6 as a structuring agent
	Reference:	Microporous Mesoporous Mat., 42, 177-189 (2001)
	Method:	relative intensities, average bond angles
	Figure:	Figures 7 and 8

Crystal Structure

	Authors:	Paillaud, J.-L., Caullet, P., Schreyeck, L. and Marler, B.
	Title:	Mu-13: a new AlPO₄ prepared with 4,13-diaza-18-crown-6 as a structuring agent
	Reference:	Microporous Mesoporous Mat., 42, 177-189 (2001)

Digitization and Modeling of Spectrum

	To reference this collection of solid-state NMR spectra, we suggest:
	Authors:	Brouwer, D.H. and White, A.L.
	Title:	A comprehensive collection of solid-state ³¹P NMR spectra of aluminophosphate zeolites.
	Reference:	Microporous Mesoporous Mat., 337, 111934 (2022)

Spectrum information

	Obs. freq.	161.97 MHz (Field = 9.4 Tesla)
	Pulse sequence	single pulse
	MAS frequency	8 kHz
	Spectrum	Digitized and processed by Brouwer Lab, Redeemer University
	Data processing	Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook
	Comment	Peak assignments are based on relative peak areas and average bond angles determined from a PXRD structure

Chemical Formula

|Kr22|₂ [Al₄₅P₄₅O₁₈₀]₂-MSO
Kr22 = C₁₂H₂₆N₂O₄ = kryptofix 22
= 1,4,10,13-tetraoxa-7,16-diazacyclooctadecane3D (stick drawing)

Downloads

	Download digitized spectrum in JCAMP-DX format (This file includes also the data listed on this page)
	Download all lines from the above plot in .csv format (This file contains only the plotted data)