Database of Zeolite Structures
 
Framework Type AFO
31P MAS NMR spectrum of calcined AlPO-41


Note: Toggle plots by clicking on the legend

Peak
Q-type
Chemical Shift
Relative
Peak Width
Peak Shape
Label
(ppm)
Peak Area
(ppm)
(x)L (1-x)G
A
Q4(4Al)
-31.38
1.000
2.00
0.234
B
Q4(4Al)
-30.36
1.000
2.00
0.234
C
Q4(4Al)
-30.01
1.000
2.00
0.234
D
Q4(4Al)
-29.71
1.000
2.00
0.234
E
Q4(4Al)
-28.48
1.000
2.00
0.234


References
Spectrum

  Authors: Caldarelli, S., Meden, A., Tuel, A.
  Title: Solid-state nuclear magnetic resonance study of the microporous aluminophosphate AlPO4-41
  Reference: J. Phys. Chem. B, 103, 5477-5487 (1999)
  Figure: Figure 3a  

Crystal Structure

  Authors: Kirchner, R.M. and Bennett, J.M.
  Title: The structure of calcined AlPO4-41: A new framework topology containing one-dimensional 10-ring pores
  Reference: Zeolites, 14, 523-528 (1994)

Digitization and Modeling of Spectrum

  To reference this collection of solid-state NMR spectra, we suggest:
  Authors: Brouwer, D.H. and White, A.L.
  Title: A comprehensive collection of solid-state 31P NMR spectra of aluminophosphate zeolites.
  Reference: Microporous Mesoporous Mat., 337, 111934 (2022)
Spectrum information

  Obs. freq. 161.2 MHz (Field = 9.3 Tesla)
  Pulse sequence single pulse
  MAS frequency 14 kHz
  Spectrum Digitized and processed by Brouwer Lab, Redeemer University
  Data processing Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook
 
  CommentPeak assignments are not available

Chemical Formula

  [Al - P - O]-AFO

Downloads

  Download digitized spectrum in JCAMP-DX format
(This file includes also the data listed on this page)
  Download all lines from the above plot in .csv format
(This file contains only the plotted data)

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